HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1,3-Dimethyl-5-nitroisoquinoline → 1,3-Dimethylisoquinolin-5-amine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1,3-Dimethyl-5-nitroisoquinoline | HCID 57456780 | — |
| Katalysator | Palladium | HCID 23938 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Produkt | 1,3-Dimethylisoquinolin-5-amine | HCID 22337624 | — |
Reaktionsschritte
A solution of D3 (2.01 g, 9.94 mM) and 10% palladium on charcoal (1 g) in methanol was hydrogenated at atmospheric pressure for 1 h. The catalyst was filtered off and the filtrate concentrated under reduced pressure to afford the title compound as an off white solid.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08063078B2 |
| Quelldatensatz | uspto-grants-2011_11 |
| ORD ID | ord-8b298f91f862430fb1b4d0d9f7fe359c |
| Quellennotiz | uspto-grants-2011_11 |