HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Benzylamine → Ethyl 3-(benzylamino)-3-methylbutanoate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Benzylamine | HCID 7504 | — |
| Edukt | Ethyl 3,3-dimethylacrylate | HCID 12516 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | Ethyl 3-(benzylamino)-3-methylbutanoate | HCID 288946 | 21,1% |
Reaktionsschritte
A solution of ethyl 3,3-dimethylacrylate (19.3 g, 0.151 mol) in EtOH (150 mL) was added benzylamine (16.2 g, 0.151 mol) and refluxed for 24 h. The reaction mixture was concentrated in vacuo. The distillation of the residue gave ethyl 3-benzylamino-3-methylbutyrate as a colorless oil (7.48 g, 21%).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08063221B2 |
| Quelldatensatz | uspto-grants-2011_11 |
| ORD ID | ord-319b932dd8ae4c888979a6e751abcd91 |
| Quellennotiz | uspto-grants-2011_11 |