Potassium Carbonate → HCID 22467254, Verbindung

HRID 561793Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 561793
C([C:3]1[C:8]([CH3:9])=[C:7]([Cl:10])[CH:6]=[CH:5][C:4]=1[OH:11])C.C(=O)([O-])[O-].[K+].[K+].Br[CH2:19][CH2:20][O:21][CH3:22]>CC(C)=O>[Cl:10][C:7]1[CH:6]=[CH:5][C:4]([O:11][CH2:19][CH2:20][O:21][CH3:22])=[CH:3][C:8]=1[CH3:9]

Komponenten

5

Edukt 3

HCID 11430Potassium CarbonateHCID 809722-Bromoethyl methyl etherHCID 22134509Ethyl 4-chloro-3-methylphenol

Produkt 1

HCID 22467254HCID 22467254, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 180AcetoneLösungsmittel

Versuchsvorschrift

To a solution of ethyl 4-chloro-3-methylphenol (1 eq.) in acetone (0.2 M) was added potassium carbonate (5 eq.) and 1-bromo-2-methoxyethane (1.3 eq.). The resulting suspension was refluxed for 25 h. The insolubles were removed via filtration and the filtrate was concentrated in vacuo to furnish the title compound.

Aufarbeitung

  1. temperatureThe resulting suspension was refluxed for 25 h
  2. customThe insolubles were removed via filtration
  3. concentrationthe filtrate was concentrated in vacuo

Quellen und Nachweise

ORD-Eintrag
ord-224af951c7104183870510e77339fa69
Quelldatensatz
uspto-grants-2011_11
Patentnummer
US08063105B2

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