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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 561893Erstellt: 26. Oktober 2026

Ethyl cyanoacetate → Poly(oxy-1,2-ethanediyl), alpha-[4-(2-cyano-3-ethoxy-3-oxo-1-propenyl)phenyl]-omega-hydroxy-

https://huagongshe.com/reaction/561893

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktEthyl cyanoacetateHCID 7764—
EduktHexaneHCID 8058—
EduktBenzaldehyde, 4-(2-hydroxyethoxy)-HCID 89178—
LösungsmittelEthanolHCID 702—
ProduktPoly(oxy-1,2-ethanediyl), alpha-[4-(2-cyano-3-ethoxy-3-oxo-1-propenyl)phenyl]-omega-hydroxy-HCID 50742116—

Reaktionsschritte

Ethyl cyanoacetate (1.1 eq.) and 4-(2-hydroxyethoxy)benzaldehyde (1 eq.) were combined in ethanol (1.2 M). The reaction mixture was stirred at RT for 48. To this was then added an equal volume of hexane and the title compound was isolated by filtration as a pale yellow solid.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS08063105B2
Quelldatensatzuspto-grants-2011_11
ORD IDord-1040e73697ea45ebbefdd1e7f8935a97
Quellennotizuspto-grants-2011_11