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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 56215Erstellt: 24. Oktober 2026

2-Furanpropionic acid → 3-(Oxolan-2-yl)propanoic acid

https://huagongshe.com/de/reaction/56215

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt2-Furanpropionic acidHCID 70286—
KatalysatorPalladiumHCID 23938—
LösungsmittelMethanolHCID 887—
Produkt3-(Oxolan-2-yl)propanoic acidHCID 263161—

Reaktionsbedingungen

Temperatur60 °C

Reaktionsschritte

A mixture of 3-(furan-2-yl)propanoic acid (11.0 g, 80.0 mmol) and Pd/C (1.1 g, 10%) in MeOH (110 mL) was stirred at 60° C. under 30 bar of H2 overnight. The mixture was then filtered and the filtrate was concentrated in vacuo to give the title compound, which was used for next step without further purification.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS09434695B2
Quelldatensatzuspto-grants-2016_09
ORD IDord-9f3c11f0258740c08bd5d0b5b6d2e178
Quellennotizuspto-grants-2016_09