Sulfur dichloride → 2-(Cyclohexyloxy)acetyl chloride

Beteiligte Stoffe

Reaktionsschritte

A mixture of 2-(cyclohexyloxy)acetic acid (0.90 g, 5.69 mmol) and dichlorosulfane (10 mL) was refluxed for 2 h. The mixture was cooled to rt and concentrated in vacuo to give the title compound as yellow oil, which was used for next step without further purification.

Herkunft & Nachweise