HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Dimethyldioxirane → 8-Benzyloxy-3-methyl5-oxiranyl-1H-quinolin-2-one
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Dimethyldioxirane | HCID 115197 | — |
| Edukt | 8-Benzyloxy-3-methyl-5-vinyl-1H-quinolin-2-one | HCID 22499178 | — |
| Lösungsmittel | Acetone | HCID 180 | — |
| Produkt | 8-Benzyloxy-3-methyl5-oxiranyl-1H-quinolin-2-one | HCID 57494231 | — |
Reaktionsschritte
To 8-benzyloxy-3-methyl-5-vinyl-1H-quinolin-2-one (300 mg) is added to a 0.1M solution of dimethyldioxirane in acetone (12.4 mL). After stirring at room temperature for 2 hours, the solvent is removed in vacuo to yield the product.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08067437B2 |
| Quelldatensatz | uspto-grants-2011_11 |
| ORD ID | ord-3b06ed7260654a95b9d202fd1a4993f3 |
| Quellennotiz | uspto-grants-2011_11 |