HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 562902Erstellt: 25. Oktober 2026
Sodium Azide → Methyl 2-(4-azido-3-cyanophenyl)isonicotinate
https://huagongshe.com/reaction/562902
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Sodium Azide | HCID 33557 | — |
| Edukt | Methyl 2-(3-cyano-4-fluorophenyl)isonicotinate | HCID 66995083 | — |
| Lösungsmittel | Dimethylformamide | HCID 6228 | — |
| Produkt | Methyl 2-(4-azido-3-cyanophenyl)isonicotinate | HCID 86626138 | — |
Reaktionsschritte
Methyl 2-(3-cyano-4-fluorophenyl)isonicotinate and sodium azide were dissolved in a DMF solution, followed by stirring at 50° C. for 4 hours to obtain methyl 2-(4-azido-3-cyanophenyl)isonicotinate. NMRC: 7.38 (1H, d), 7.84 (1H, dd), 8.46 (1H, d)
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US08067446B2 |
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| Quelldatensatz | uspto-grants-2011_11 |
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| ORD ID | ord-2b602ad16214468eb29c347fe90aa8f1 |
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| Quellennotiz | uspto-grants-2011_11 |
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