HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Ethanol → Ethyl 3-bromo-4-methoxyphenylacetate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Ethanol | HCID 702 | — |
| Edukt | 3-Bromo-4-methoxyphenylacetic acid | HCID 136615 | — |
| Lösungsmittel | Sulfuric Acid | HCID 1118 | — |
| Produkt | Ethyl 3-bromo-4-methoxyphenylacetate | HCID 57419861 | — |
Reaktionsschritte
A solution of 3-bromo-4-methoxyphenylacetic acid (3.0 g, 12.2 mmol) in EtOH and sulfuric acid was stirred at 100° C. for 2 hours. The mixture was concentrated and partitioned between EtOAc and H2O, and the organic layer was separated to give the title compound.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08067445B2 |
| Quelldatensatz | uspto-grants-2011_11 |
| ORD ID | ord-e3d6e9063a61482c9b1a0e69f21c57b7 |
| Quellennotiz | uspto-grants-2011_11 |