N-Methylbenzylamine → N-methoxyethyl-N-methylbenzylamine
Reaktionsgleichung
[CH3:1][NH:2][CH2:3][C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1.[CH3:10][O:11][CH2:12][CH2:13]Br>C(O)C>[CH3:10][O:11][CH2:12][CH2:13][N:2]([CH2:3][C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1)[CH3:1]Komponenten
4
Edukt 2
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
The synthesis of BnMO was carried out in a manner similar to that of BnEO (process 2) using N-methylbenzylamine (15 mL, 0.116 mol), bromoethyl methyl ether (12 mL, 0.116×1.1 mmol), and ethanol (200 mL) as a solvent. BnMO (12.09 g, 67.46 mmol, yield 58%) was obtained as a pale yellow clear liquid.
Aufarbeitung
- customThe synthesis of BnMO
- customBnMO (12.09 g, 67.46 mmol, yield 58%) was obtained as a pale yellow clear liquid
Quellen und Nachweise
- ORD-Eintrag
- ord-2fb5ed35fdea45d58a00e27cecf3253d
- Quelldatensatz
- uspto-grants-2011_11
- Patentnummer
- US08067595B2
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