HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2,6-Difluorobenzoyl chloride → 2-(2,6-Difluoro-phenyl)-5-methyl-benzo[d][1,3]oxazin-4-one
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2,6-Difluorobenzoyl chloride | HCID 87438 | — |
| Edukt | 6-Methylanthranilic acid | HCID 151210 | — |
| Edukt | 6-Acetamido-(2,6-difluoro-phenyl)-benzo[d][1,3]oxazin-4-one | HCID 9948813 | — |
| Lösungsmittel | Toluene triethylamine | HCID 22504574 | — |
| Produkt | 2-(2,6-Difluoro-phenyl)-5-methyl-benzo[d][1,3]oxazin-4-one | HCID 21262479 | — |
Reaktionsschritte
2-Amino-6-methylbenzoic acid (0.498 g), 2,6-difluorobenzoyl chloride (0.93 mL) and triethyl amine/toluene (1/1) (20 mL) were reacted as described under (10).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06180625B2 |
| Quelldatensatz | uspto-grants-2001_01 |
| ORD ID | ord-3b042ae8eaad4006bc28228c70a460e6 |
| Quellennotiz | uspto-grants-2001_01 |