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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 567998Erstellt: 25. Oktober 2026

1-Amino-2-naphthol → N-(2-hydroxynaphthyl) N'-(2-bromo phenyl) urea

https://huagongshe.com/reaction/567998

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt1-Amino-2-naphtholHCID 14535—
Edukt2-Bromophenyl isocyanateHCID 137097—
ProduktN-(2-hydroxynaphthyl) N'-(2-bromo phenyl) ureaHCID 220113188,4%

Reaktionsschritte

The urea was prepared from 1-amino 2-hydroxynapthalene(195 mg, 1 mmol) and 2-bromophenylisocyanate(1 mmol) by general Method B. It was purified by dilution with methylene chloride and precipitation with hexane. Filtering afforded the title compound(0.030 g, 8%). EI-MS m/z 357(M+H)+.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS06180675B2
Quelldatensatzuspto-grants-2001_01
ORD IDord-ca3cbc344ed34db7bc3af4ab29795a80
Quellennotizuspto-grants-2001_01