N-[3-(1H-imidazol-1-yl)propyl]glycinamide → HCID 178521282, Verbindung
Reaktionsgleichung
[N:1]1([CH2:6][CH2:7][CH2:8][NH:9][C:10](=[O:13])[CH2:11][NH2:12])[CH:5]=[CH:4][N:3]=[CH:2]1.I.CS[C:17]1[C:25]2[CH:26]=[CH:27][CH:28]=[C:23]3[C:24]=2[C:19](=[CH:20][CH:21]=[CH:22]3)[N:18]=1>C(O)C>[N:18]1[C:19]2[C:24]3[C:23](=[CH:28][CH:27]=[CH:26][C:25]=3[C:17]=1[NH:12][CH2:11][C:10]([NH:9][CH2:8][CH2:7][CH2:6][N:1]1[CH:5]=[CH:4][N:3]=[CH:2]1)=[O:13])[CH:22]=[CH:21][CH:20]=2Komponenten
4
Edukt 2
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
A mixture of 3.7 g of N-[3-(1H-imidazol-1-yl)propyl]glycinamide, 425 ml of ethanol, and 5.0 g of 2-(methylthio)benz[cd]indole hydroiodide was reacted as described in Example 19, giving 2.2 g of the desired product, mp 145°-146° C.