HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Thionyl Chloride → p-(1-Methyl-heptyloxy)benzoic acid chloride
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Thionyl Chloride | HCID 24386 | — |
| Edukt | p-(1-Methyl-heptyloxy)benzoic acid | HCID 13878419 | — |
| Produkt | p-(1-Methyl-heptyloxy)benzoic acid chloride | HCID 13878422 | 93% |
Reaktionsschritte
Thionyl chloride (51.2 g, 0.43 mol) was added to optically active p-(1-methyl-heptyloxy)benzoic acid (90.0 g, 0.36 mol), followed by refluxing the mixture for about 2 hours, thereafter completely removing excess thionyl chloride by distillation under reduced pressure to obtain optically active p-(1-methyl-heptyloxy)benzoic acid chloride (90.0 g).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04729847 |
| Quelldatensatz | uspto-grants-1988_03 |
| ORD ID | ord-a514f906415d486db0b095e432061e79 |
| Quellennotiz | uspto-grants-1988_03 |