4,4'-Thiodianiline → Toluene heptane
Reaktionsgleichung
NC1C=CC(SC2C=CC(N)=CC=2)=CC=1.[C:16]1([C:22]#[C:23]C2C=C(C=CC=2)C=O)[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1>C(O)C>[CH3:23][CH2:22][CH2:16][CH2:17][CH2:18][CH2:19][CH3:20].[C:16]1([CH3:22])[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1Komponenten
4
Edukt 2
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
Using a procedure similar to that described in Example 5, 3.4 g (0.016 mol) of 4-aminophenylsulfide was reacted with 6.6 g (0.032 mol) of 3-phenylethynylbenzaldehyde in 75 ml of ethanol. The product precipitates as a yellow solid which was recrystallized from heptane/toluene (8.9 g, 0.015 mol, 94% yield).
Aufarbeitung
- customThe product precipitates as a yellow solid which
Quellen und Nachweise
- ORD-Eintrag
- ord-5b812541eafa4f43b1678de1e54ddb47
- Quelldatensatz
- uspto-grants-1988_03
- Patentnummer
- US04730032
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