HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Ammonia → Morpholine-4-carboxamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Ammonia | HCID 222 | — |
| Edukt | 4-Morpholinecarbonyl chloride | HCID 84810 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Produkt | Morpholine-4-carboxamide | HCID 75088 | — |
Reaktionsschritte
A solution of morpholine-4-carbonyl chloride (2.0 g) in methanol (10 mL) and 7 N NH3 in methanol (5 mL) was stirred at 45° C. overnight. The mixture was concentrated to give a solid, which was dried under vacuum.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US09034875B2 |
| Quelldatensatz | uspto-grants-2015_05 |
| ORD ID | ord-bc64eee410bf4511854d76a992fb5970 |
| Quellennotiz | uspto-grants-2015_05 |