HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 57550Erstellt: 24. Oktober 2026
N-methyl-5-nitro-N-(tetrahydro-2H-pyran-4-yl)pyridin-2-amine → N2-methyl-N2-(tetrahydro-2H-pyran-4-yl)-2,5-Pyridinediamine
https://huagongshe.com/de/reaction/57550
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | N-methyl-5-nitro-N-(tetrahydro-2H-pyran-4-yl)pyridin-2-amine | HCID 71113503 | — |
| Katalysator | Palladium | HCID 23938 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Produkt | N2-methyl-N2-(tetrahydro-2H-pyran-4-yl)-2,5-Pyridinediamine | HCID 43610738 | — |
Reaktionsschritte
To a solution of N-methyl-5-nitro-N-(tetrahydro-2H-pyran-4-yl)pyridin-2-amine (217 mg, 0.92 mmol) in MeOH (30 mL) was added Pd/C (0.5 g). The mixture was stirred for 3 hours at 20° C. under 1 atm. H2. The reaction was filtered and concentrated to give dark red oil. MS (m/z): 208 (M+H)+
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US09434726B2 |
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| Quelldatensatz | uspto-grants-2016_09 |
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| ORD ID | ord-3bdf9a7e1e4441f8bbbb21f22db9e522 |
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| Quellennotiz | uspto-grants-2016_09 |
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