HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
L-Aspartic Acid → HCID 178512698, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | L-Aspartic Acid | HCID 5960 | — |
| Edukt | HCID 178418935 | HCID 178418935 | — |
| Lösungsmittel | Dichloromethane | HCID 6344 | — |
| Produkt | HCID 178512698 | HCID 178512698 | — |
Reaktionsschritte
A mixture of 0.56 g (0.166 cmole) of famotidine and 0.222 g (0.166 cmole) of aspartic acid was suspended in dichloromethane (10 ml). The mixture was stirred for 3 hours at room temperature, was filtered, washed with dichloromethane and dried. Weight: 0.782 g. Quantitative yield. Stereoscopically homogenous white microcrystalline solid, similar to milky quartz. Slightly bitter taste. M.P.: 165°-170° C. IR FIG. 2.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04749790 |
| Quelldatensatz | uspto-grants-1988_06 |
| ORD ID | ord-f1b01b4e29a740aa9b69fbc4007a5bb9 |
| Quellennotiz | uspto-grants-1988_06 |