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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 581875Erstellt: 25. Oktober 2026

5-Ethyl-6-(3,5-dimethylphenoxy)-2,4-pyrimidinedione → 1-{[3,4-Di(hydroxymethyl)cyclopent-1-en-1-yl]methyl}-5-ethyl-6-(3,5-dimethylphenoxy)-2,4-pyrimidinedione

https://huagongshe.com/reaction/581875

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt5-Ethyl-6-(3,5-dimethylphenoxy)-2,4-pyrimidinedioneHCID 10923266—
Edukt[3,4-Di(t-butyldimethylsilyloxymethyl)cyclopent-1-en-1-yl]methyl bromideHCID 54350482—
Produkt1-{[3,4-Di(hydroxymethyl)cyclopent-1-en-1-yl]methyl}-5-ethyl-6-(3,5-dimethylphenoxy)-2,4-pyrimidinedioneHCID 5377078617,9%

Reaktionsschritte

5-Ethyl-6-(3,5-dimethylphenoxy)-2,4-pyrimidinedione and [3,4-di(t-butyldimethylsilyloxymethyl)cyclopent-1-en-1-yl]methyl bromide were reacted by the same method with example 28 to obtain the titled compound (42 mg).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05922727
Quelldatensatzuspto-grants-1999_07
ORD IDord-1af4f80f76084b64ab9733192e2b0430
Quellennotizuspto-grants-1999_07