5-Isopropyl-6-(3,5-dimethylphenyl)thio-2,4-pyrimidinedione → 1-(2-Cyclopent-3-en-1-ylethyl)-6-(3,5-dimethylphenyl)sulfanyl-5-isopropyl-pyrimidine-2,4-dione

HRID 581883

Reaktionsgleichung

Reaktionsgleichung von HRID 581883
[CH:1]([C:4]1[C:5](=[O:20])[NH:6][C:7](=[O:19])[NH:8][C:9]=1[S:10][C:11]1[CH:16]=[C:15]([CH3:17])[CH:14]=[C:13]([CH3:18])[CH:12]=1)([CH3:3])[CH3:2].C1(C)C(S(O[CH2:31][CH2:32][CH:33]2[CH2:37][CH:36]=[CH:35][CH2:34]2)(=O)=O)=CC=CC=1>>[CH:33]1([CH2:32][CH2:31][N:8]2[C:9]([S:10][C:11]3[CH:12]=[C:13]([CH3:18])[CH:14]=[C:15]([CH3:17])[CH:16]=3)=[C:4]([CH:1]([CH3:3])[CH3:2])[C:5](=[O:20])[NH:6][C:7]2=[O:19])[CH2:37][CH:36]=[CH:35][CH2:34]1

Komponenten

3

Edukt 2

HCID 104937275-Isopropyl-6-(3,5-dimethylphenyl)thio-2,4-pyrimidinedioneHCID 867542212-(Cyclopent-3-en-1-yl)ethyl toluenesulfonate

Produkt 1

HCID 452690751-(2-Cyclopent-3-en-1-ylethyl)-6-(3,5-dimethylphenyl)sulfanyl-5-isopropyl-pyrimidine-2,4-dioneAusbeute 34,8 %

Versuchsvorschrift

5-Isopropyl-6-(3,5-dimethylphenylthio)-2,4-pyrimidinedione and 2-(cyclopent 3-en-1-yl)ethyl toluenesulfonate were reacted by the same method with example 35 to obtain the titled compound (134 mg).

Quellen und Nachweise

ORD-Eintrag
ord-adbd1622bf1e41b9a63e8c60ac58fac9
Quelldatensatz
uspto-grants-1999_07
Patentnummer
US05922727

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