HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3-(3-Nitrophenyl)pyridine → 3-(Pyridin-3-yl)aniline
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3-(3-Nitrophenyl)pyridine | HCID 12181327 | — |
| Katalysator | Nickel | HCID 935 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | 3-(Pyridin-3-yl)aniline | HCID 459521 | — |
Reaktionsschritte
3-(3-pyridyl)-nitrobenzene (9.1 g, 45.5 mmol) in ethanol (125 ml) is hydrogenated at ambient pressure for 1.75 hours using Raney Nickel as the catalyst. Filtration of the resulting solution through celite followed by evaporation of solvent quantitatively yields 3-(3-pyridyl)aniline.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05922724 |
| Quelldatensatz | uspto-grants-1999_07 |
| ORD ID | ord-e2c51de4f901493c8a5c8e21efe583c1 |
| Quellennotiz | uspto-grants-1999_07 |