HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Dimethyl Sulfide → (2-Ethoxy-2-oxoethyl)dimethylsulphonium bromide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Dimethyl Sulfide | HCID 1068 | — |
| Edukt | Ethyl bromoacetate | HCID 7748 | — |
| Lösungsmittel | Acetone | HCID 180 | — |
| Produkt | (2-Ethoxy-2-oxoethyl)dimethylsulphonium bromide | HCID 78861 | — |
Reaktionsschritte
A solution of ethyl bromoacetate (265 g) and dimethyl sulfide (114 g) in acetone (500 mL) was stirred at room temperature. After three days, the title compound was isolated by filtration of the reaction mixture. Melting point 88-90° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05925782 |
| Quelldatensatz | uspto-grants-1999_07 |
| ORD ID | ord-950d9b632701446f88a52f5033b6d2e5 |
| Quellennotiz | uspto-grants-1999_07 |