HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
12-Methoxydodecanoate → 12-Methoxydodecanoyl chloride
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 12-Methoxydodecanoate | HCID 1420 | — |
| Edukt | Oxalyl chloride | HCID 65578 | — |
| Edukt | 12-Methoxy-N-(phenylmethyl)dodecanamide | HCID 9797119 | — |
| Lösungsmittel | Toluene | HCID 1140 | — |
| Produkt | 12-Methoxydodecanoyl chloride | HCID 19611759 | — |
Reaktionsschritte
Reaction Scheme 4 illustratively shows the preparation of 12-methoxy-N-(phenyl-methyl)dodecanamide wherein 12-methoxydodecanoic acid (8) is treated with oxalyl chloride in anhydrous toluene to form 12-methoxydodecanoyl chloride (9) which in turn reacts with benzylamine in methylene chloride to give the desired fatty acid amide (10).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05929110 |
| Quelldatensatz | uspto-grants-1999_07 |
| ORD ID | ord-18409ab56e9146fa80ab1f57f2103424 |
| Quellennotiz | uspto-grants-1999_07 |