N,N-Diallylacrylamide → HCID 70054299, Verbindung
Reaktionsgleichung
[CH3:1][O:2][C:3](=[O:31])[C:4]1[CH:9]=[C:8](Br)[CH:7]=[C:6]([CH3:11])[C:5]=1[N:12]([S:20]([C:23]1[CH:28]=[CH:27][C:26]([O:29][CH3:30])=[CH:25][CH:24]=1)(=[O:22])=[O:21])[CH2:13][C:14]1[CH:15]=[N:16][CH:17]=[CH:18][CH:19]=1.[CH2:32]([N:35]([CH2:40][CH:41]=[CH2:42])[C:36](=[O:39])[CH:37]=[CH2:38])[CH:33]=[CH2:34]>>[CH3:1][O:2][C:3](=[O:31])[C:4]1[CH:9]=[C:8]([CH:38]=[CH:37][C:36](=[O:39])[N:35]([CH2:32][CH:33]=[CH2:34])[CH2:40][CH:41]=[CH2:42])[CH:7]=[C:6]([CH3:11])[C:5]=1[N:12]([S:20]([C:23]1[CH:28]=[CH:27][C:26]([O:29][CH3:30])=[CH:25][CH:24]=1)(=[O:22])=[O:21])[CH2:13][C:14]1[CH:15]=[N:16][CH:17]=[CH:18][CH:19]=1Komponenten
3
Versuchsvorschrift
In the same manner as described in Example 203, 550.4 mg (1.0 mmol) of the product of Example 89 and 453.6 mg (3.0 mmol) of N,N-diallylacrylamide provided 309 mg (53%) of the desired product as a yellow gum. Electrospray Mass Spec 576(M+H).
Quellen und Nachweise
- ORD-Eintrag
- ord-c2edf6d078ad49e789bbb522a4a89f22
- Quelldatensatz
- uspto-grants-1999_07