HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Dimethylformamide → HCID 178424083, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Dimethylformamide | HCID 6228 | — |
| Edukt | 2-Methylbenzonitrile | HCID 10721 | — |
| Edukt | Ammonium Chloride | HCID 25517 | — |
| Edukt | Sodium Azide | HCID 33557 | — |
| Produkt | HCID 178424083 | HCID 178424083 | — |
Reaktionsschritte
Tolunitrile (103 mg, 1.0 mmol) was refluxed with NH4Cl (70 mg, 1.3 mmol), and NaN3 (85 mg, 1.3 mmol) in 3 mL of DMF overnight. The resulting 5-p-tolyl tetrazole was purified via RP-HPLC.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06924284B2 |
| Quelldatensatz | uspto-grants-2005_08 |
| ORD ID | ord-a861a45610ea48e08c32a36e0d3d9260 |
| Quellennotiz | uspto-grants-2005_08 |