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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 585364Erstellt: 25. Oktober 2026

3-Methoxybenzoic Acid → 1-(3-Methoxybenzoyl)-2-methyl-1,2,3,4-tetrahydro-4-quinolinol

https://huagongshe.com/reaction/585364

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt3-Methoxybenzoic AcidHCID 11461—
Edukt1,2,3,4-Tetrahydro-2-methyl-4-quinolinolHCID 147634—
Produkt1-(3-Methoxybenzoyl)-2-methyl-1,2,3,4-tetrahydro-4-quinolinolHCID 2233923227%

Reaktionsschritte

Starting with 2-methyl-1,2,3,4-tetrahydro-4-quinolinol (3.00 g, 18.3 mmol) synthesized in the published manner and 3-methoxybenzoic acid (3.34 g, 22.0 mmol), the same procedure as shown in Reference Example 19 was repeated to give the titled compound (1.45 g, yield: 27%) as a white crystal. (cis:trans=1:1)

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS06930104B2
Quelldatensatzuspto-grants-2005_08
ORD IDord-5b593778956443bd8eafd7c9b3e79dea
Quellennotizuspto-grants-2005_08