HCID 86759825, Verbindung → HCID 131725086, Verbindung

HRID 586668Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 586668
[CH3:1][O:2][CH2:3][C@@H:4]1[C@H:6](/[CH:7]=[CH:8]/[C:9](/[CH3:16])=[CH:10]/[C:11]([O:13][CH2:14][CH3:15])=[O:12])[C@@:5]1([CH3:31])[C:17]1[CH:26]=[CH:25][C:24]2[C:23]([CH3:28])([CH3:27])[CH2:22][CH2:21][C:20]([CH3:30])([CH3:29])[C:19]=2[CH:18]=1.[CH2:32](OC[C@@H]1[C@@H](C=O)[C@@]1(C)C1C=CC2C(C)(C)CCC(C)(C)C=2C=1)C>>[CH2:1]([O:2][CH2:3][C@@H:4]1[C@@H:6](/[CH:7]=[CH:8]/[C:9](/[CH3:16])=[CH:10]/[C:11]([O:13][CH2:14][CH3:15])=[O:12])[C@:5]1([CH3:31])[C:17]1[CH:26]=[CH:25][C:24]2[C:23]([CH3:28])([CH3:27])[CH2:22][CH2:21][C:20]([CH3:30])([CH3:29])[C:19]=2[CH:18]=1)[CH3:32]

Komponenten

3

Edukt 2

HCID 86759825HCID 86759825, VerbindungHCID 131725081HCID 131725081, Verbindung

Produkt 1

HCID 131725086HCID 131725086, VerbindungAusbeute 73 %

Versuchsvorschrift

Following a procedure similar to that for the preparation of Compound 16a but using Intermediate 15b as the starting material afforded the title compound (35 mg, 73% yield) as a white solid:

Quellen und Nachweise

ORD-Eintrag
ord-023c98b44191452794df4331035896f8
Quelldatensatz
uspto-grants-2005_08
Patentnummer
US06936636B2

Notizen zur Reaktion

Wird geladen…