HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Bromopropane → Methyl 4-(5-bromo-2-cyano-1-methoxy-1-oxopentan-2-yl)benzoate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Bromopropane | HCID 6358 | — |
| Edukt | Dimethyl Carbonate | HCID 12021 | — |
| Edukt | Sodium hydride | HCID 24758 | — |
| Edukt | 3,4-Dimethoxybenzeneacetonitrile | HCID 66727 | — |
| Edukt | Methyl 4-(cyanomethyl)benzoate | HCID 848548 | — |
| Edukt | Sodium bis(trimethylsilyl)amide | HCID 2724254 | — |
| Produkt | Methyl 4-(5-bromo-2-cyano-1-methoxy-1-oxopentan-2-yl)benzoate | HCID 59419916 | — |
Reaktionsschritte
For Step 1, methyl 4-(cyanomethyl)benzoate was substituted for (3,4-Dimethoxyphenyl)acetonitrile and dimethyl carbonate was substituted for 2-bromopropane. For Step 2, sodium hydride was substituted for NaHMDS.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US09227918B2 |
| Quelldatensatz | uspto-grants-2016_01 |
| ORD ID | ord-93172768202b488bbf9cd50f45bba093 |
| Quellennotiz | uspto-grants-2016_01 |