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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 59011Erstellt: 26. Oktober 2026

Ammonia → HCID 178463316, Verbindung

https://huagongshe.com/reaction/59011

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktAmmoniaHCID 222—
EduktEthanolHCID 702—
EduktOrcinolHCID 10436—
EduktAmmonium PersulfateHCID 62648—
EduktN-Ethyl-N-isopropyl-p-phenylenediamine hydrochlorideHCID 16211123—
LösungsmittelWaterHCID 962—
ProduktHCID 178463316HCID 178463316—

Reaktionsschritte

To a solution of 0.002 mol (429 mg) of N-ethyl-N-isopropyl-4-aminoaniline hydrochloride and 0.001 mol (124 mg) of orcinol in 2 ml of water and 6 ml of ethanol brought to a pH of 9.5 with a solution of 20% aqueous ammonia, 0.002 mol (456 mg) of ammonium persulfate dissolved in 1 ml of water is added dropwise. The temperature is held below 30° C. during the addition. At the end of the addition, the precipitate formed is filtered and washed with water.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS09439844B2
Quelldatensatzuspto-grants-2016_09
ORD IDord-4cf052ea8c254f09bf3992e6e71354c9
Quellennotizuspto-grants-2016_09