Hydrogen Peroxide → Ethanamine, N,N-diethyl-, N-oxide

HRID 596920

Reaktionsgleichung

Reaktionsgleichung von HRID 596920
OO.[OH:3][N:4]([CH2:7][CH3:8])[CH2:5][CH3:6].C[I:10].[CH2:11]([N:13]([CH2:16][CH3:17])[CH2:14]C)[CH3:12]>>[CH2:5]([N+:4]([O-:3])([CH2:11][CH3:12])[CH2:7][CH3:8])[CH3:6].[I-:10].[CH2:11]([N+:13]([CH2:16][CH3:17])([CH3:14])[OH:3])[CH3:12]

Komponenten

6

Edukt 4

HCID 784Hydrogen PeroxideHCID 6328Methyl iodideHCID 8471TriethylamineHCID 19463Diethylhydroxylamine

Produkt 2

HCID 123168Ethanamine, N,N-diethyl-, N-oxideHCID 21449162Diethylmethylhydroxyammonium iodide

Versuchsvorschrift

Triethylamine oxide and diethylmethylhydroxyammonium iodide were prepared in situ starting triethylamine and 30l% by weight aqueous hydrogen peroxide, and hydroxydiethylamine and methyl iodide.

Quellen und Nachweise

ORD-Eintrag
ord-fb94304a4412419faac8b419c127907e
Quelldatensatz
uspto-grants-1977_03
Patentnummer
US04012430

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