HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Borane → 1H-1,4-Benzodiazepine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Borane | HCID 6331 | — |
| Edukt | N,N-diethyl-4-methyl-8-fluoro-6-(o-fluorophenyl)-4H-s-triazolo[4,3-a]-[1,4]benzodiazepine-1-acetamide | HCID 21449044 | — |
| Produkt | 1H-1,4-Benzodiazepine | HCID 148431 | — |
Reaktionsschritte
In the manner given in Example 1, N,N-diethyl-4-methyl-8-fluoro-6-(o-fluorophenyl)-4H-s-triazolo[4,3-a]-[1,4]benzodiazepine-1-acetamide is reduced with borane to give 1-[2-diethylamino)ethyl]-4-methyl-8-fluoro-5,6-dihydro-6-(o-fluorophenyl)-4H-s-triazolo]4,3-a][1,4]benzodiazepine.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04012413 |
| Quelldatensatz | uspto-grants-1977_03 |
| ORD ID | ord-f28aa78997034200b083d17358eb3950 |
| Quellennotiz | uspto-grants-1977_03 |