HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
5,7-Dichlorobenzofuran → (RS)-2-[1-(5,7-Dichloro-benzofuran-2-yl)-methanoyl]-4-methyl-piperazine-1-carboxylic acid tert-butyl ester
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 5,7-Dichlorobenzofuran | HCID 90014 | — |
| Edukt | (RS)-2-(methoxy-methyl-carbamoyl)4-methyl-piperazine-1-carboxylic acid dimethyl-ethyl ester | HCID 86625772 | — |
| Produkt | (RS)-2-[1-(5,7-Dichloro-benzofuran-2-yl)-methanoyl]-4-methyl-piperazine-1-carboxylic acid tert-butyl ester | HCID 66968136 | — |
Reaktionsschritte
The title compound (0.94 g) was prepared from (RS)-2-(methoxy-methyl-carbamoyl)-4-methyl-piperazine-1-carboxylic acid dimethyl-ethyl ester, D54 (1.00 g) and 5,7-dichloro-benzofuran (0.65 g, FP1.537.206) using the method of Description 2.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07897618B2 |
| Quelldatensatz | uspto-grants-2011_03 |
| ORD ID | ord-b1994d7d8531466bbcbf9844c167d929 |
| Quellennotiz | uspto-grants-2011_03 |