HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Benzenemethanamine, 3,4-dichloro- → 4-((3,4-Dichlorobenzyl)amino)benzo[d][1,2,3]triazine-8-carboxamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Benzenemethanamine, 3,4-dichloro- | HCID 1608 | — |
| Edukt | 4-oxo-1H-1,2,3-benzotriazine-8-carboxamide | HCID 178513613 | — |
| Produkt | 4-((3,4-Dichlorobenzyl)amino)benzo[d][1,2,3]triazine-8-carboxamide | HCID 74538689 | — |
Reaktionsschritte
Compound 2 was prepared following general synthetic scheme 7 wherein (3,4-dichlorophenyl)methanamine was reacted with 4-hydroxybenzo[d][1,2,3]-triazine-8-carboxamide to give the title compound. LC-MS [350 (M+1)], 1H NMR (400 MHz, DMSO-d6): δ 9.37 (s, 1H), 9.31 (t, 1H), 8.54 (d, 1H), 8.49 (d, 1H), 8.05 (s, 1H), 8.00 (t, 1H), 7.70 (s, 1H), 7.60 (d, 1H), 7.40 (d, 1H), 4.90 (d, 1H).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US09440968B2 |
| Quelldatensatz | uspto-grants-2016_09 |
| ORD ID | ord-03bfa14da0a648559a9d736cfbfbcce9 |
| Quellennotiz | uspto-grants-2016_09 |