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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 599724Erstellt: 26. Oktober 2026

Oxygen → 4-Phenyl-3-Buten-2-one

https://huagongshe.com/reaction/599724

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktOxygenHCID 977—
Edukt4-Phenylbut-3-en-2-olHCID 15172—
KatalysatorPlatinumHCID 23939—
LösungsmittelWaterHCID 962—
Produkt4-Phenyl-3-Buten-2-oneHCID 1590987,5%

Reaktionsschritte

In an ambient pressure oxygen atmosphere, 29.2 mg of 4-phenyl-but-3-ene-2-ol and 33.9 mg of the platinum catalyst obtained in Example 1 were agitated for fifteen hours at 60° C. in 2 ml of water. The reaction mixture was subsequently extracted using ethyl acetate, and the organic layer was dried using magnesium sulfate, filtered and concentrated to obtain 25.2 mg (87% yield) of benzalacetone. The reaction equation and the analytical results of the product are shown below.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07897817B2
Quelldatensatzuspto-grants-2011_03
ORD IDord-441a9e81c2ae40b4b5312c7d92167e28
Quellennotizuspto-grants-2011_03