3-Cyanophenol → O-3-cyanophenyl dimethylthiocarbamate

Beteiligte Stoffe

Rolle	Name	HCID	Einwaage
Edukt	3-Cyanophenol	HCID 13394	—
Edukt	Potassium Hydroxide	HCID 14797	—
Edukt	Dimethylthiocarbamoyl chloride	HCID 27871	—
Produkt	O-3-cyanophenyl dimethylthiocarbamate	HCID 14795402	—

Reaktionsschritte

If the procedure described in Preparation XI is followed starting from 15 g (126.10-3 mol) of 3-hydroxybenzonitrile, 17.9 g (145.10-3 mol) of dimethylthiocarbamoyl chloride and 7.4 g (132.10-3 mol) of potassium hydroxide, 29 g (quantitative yield) of the expected product are obtained.

Herkunft & Nachweise

DOI	10.6084/m9.figshare.5104873.v1
Patentnummer	US05246961
Quelldatensatz	uspto-grants-1993_09
ORD ID	ord-b26089eaf91d4f27b4272b0ec41c29a8
Quellennotiz	uspto-grants-1993_09