HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Mercuric cyanide → 3-cyanophenyl 2,3,4-tri-O-acetyl-1,5-dithio-beta-D-xylopyranoside
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Mercuric cyanide | HCID 11591 | — |
| Edukt | 2,3,4-tri-O-acetyl-5-thio-alpha-xylopyranosyl bromide | HCID 10926314 | — |
| Edukt | 3-Sulfanylbenzonitrile | HCID 14795334 | — |
| Produkt | 3-cyanophenyl 2,3,4-tri-O-acetyl-1,5-dithio-beta-D-xylopyranoside | HCID 14795343 | — |
Reaktionsschritte
If the procedure described in Preparation I is followed starting from 9.3 g (67.10-3 mol) of 3-mercaptobenzonitrile, 18 g (73.10-3 mol) of mercuric cyanide, Hg(CN)2, and 26.14 g (73.10-3 mol) of 2,3,4-tri-O-acetyl-5-thio-α-D-xylopyranosyl bromide, 8.55 g of the expected product are obtained.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05246961 |
| Quelldatensatz | uspto-grants-1993_09 |
| ORD ID | ord-e160f17724b945938456d36adf413951 |
| Quellennotiz | uspto-grants-1993_09 |