Pentafluoroaniline → 501670-16-2

HRID 601095

Reaktionsgleichung

Reaktionsgleichung von HRID 601095
[C:1]([C:5]1[CH:10]=[C:9]([C:11]([CH3:14])([CH3:13])[CH3:12])[CH:8]=[C:7]([CH:15]=NC2C(Br)=CC=CC=2Br)[C:6]=1[OH:25])([CH3:4])([CH3:3])[CH3:2].[F:26][C:27]1[C:33]([F:34])=[C:32]([F:35])[C:31]([F:36])=[C:30]([F:37])[C:28]=1[NH2:29].C(C1C(O)=C(C=C(C(C)(C)C)C=1)C=O)(C)(C)C>>[C:1]([C:5]1[CH:10]=[C:9]([C:11]([CH3:14])([CH3:13])[CH3:12])[CH:8]=[C:7]([CH:15]=[N:29][C:28]2[C:27]([F:26])=[C:33]([F:34])[C:32]([F:35])=[C:31]([F:36])[C:30]=2[F:37])[C:6]=1[OH:25])([CH3:4])([CH3:3])[CH3:2]

Komponenten

4

Edukt 3

HCID 13040PentafluoroanilineHCID 6880233,5-Di-tert-butylsalicylaldehydeHCID 136346710HCID 136346710, Verbindung

Produkt 1

HCID 135509894501670-16-2

Versuchsvorschrift

Employing an analogous procedure to that described above for the synthesis of 2,4-bis(tert-butyl)-6-[[(2,6-dibromophenyl)imino]methyl]phenol, 2,3,4,5,6-pentafluoroaniline (0.54 g, 2.9 mmol) was added to 3,5-di-tert-butyl-2-hydroxybenzaldehyde (0.70 g, 2.9 mmol). The product was purified by recrystallisation from hot MeOH and isolated as yellow crystals.

Aufarbeitung

  1. customThe product was purified by recrystallisation from hot MeOH
  2. customisolated as yellow crystals

Quellen und Nachweise

ORD-Eintrag
ord-1224c7f7869c44258aeb252783b2e5e7
Quelldatensatz
uspto-grants-2011_03
Patentnummer
US07902308B2

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