StartseiteMCPWorkbenchSkills
StartseiteWorkbenchBenachrichtigungenMein Bereich
llms.txt · MCP-AnleitungDatenschutz · Nutzungsbedingungen · Supportv1.8.0
  1. Startseite
  2. /Reaktion

Hydrogen Peroxide → Strontium Dithiophosphate

HRID 601958
Notizen
Druckvorschau

Reaktionsgleichung

Reaktionsgleichung von HRID 601958
[P:1](=[S:5])([OH:4])([OH:3])[SH:2].[OH-].[Sr+2:7].[OH-].OO.C(OCCOCCOCCOC(=O)CCCCCCCC)(=O)CCCCCCCC>>[P:1]([O-:4])([O-:3])([S-:5])=[S:2].[Sr+2:7].[P:1]([O-:4])([O-:3])([S-:5])=[S:2].[Sr+2:7].[Sr+2:7]
KomponentenReaktionsbedingungenVersuchsvorschriftAufarbeitungQuellen und NachweiseNotizen zur Reaktion

Komponenten

5

Edukt 4

HCID 784Hydrogen PeroxideHCID 7786Ethylenebis(oxyethylene) dinonanoateHCID 87672Strontium hydroxideHCID 152119Phosphorodithioic acid

Produkt 1

HCID 86621842Strontium Dithiophosphate

Reaktionsbedingungen

Temperatur
75 °C

Versuchsvorschrift

A three neck round bottom flask was charged with 89.0 grams of the dithiophosphoric acid that was obtained from Example 9. To this was added 15.1 grams of strontium hydroxide. The reaction was heated to 75° C. for approximately 30 minutes. The reaction was attached to an aspirator to remove any water that had formed. The reaction was then allowed to cool back to 35° C., and 4.2 g of 17.5% hydrogen peroxide was added. After mixing for 2.5 hours, 11.1 grams of triethylene glycol dinonanoate was added. The reaction was then heated under vacuum and any remaining water was removed by distillation. After the temperature reached 105° C., the final product was filtered with diatomaceous earth.

Aufarbeitung

  1. customwas obtained from Example 9
  2. customto remove any water that
  3. customhad formed
  4. temperatureto cool back to 35° C.
  5. additionAfter mixing for 2.5 hours
  6. temperatureThe reaction was then heated under vacuum
  7. customany remaining water was removed by distillation
  8. customreached 105° C.
  9. filtrationthe final product was filtered with diatomaceous earth

Quellen und Nachweise

ORD-Eintrag
ord-56f11a5ad70a4d4da2d29e17f6f536f4
Quelldatensatz
uspto-grants-2011_03
DOI
10.6084/m9.figshare.5104873.v1
Patentnummer
US07902403B2

Notizen zur Reaktion

Wird geladen…

Auf dieser SeiteKomponentenReaktionsbedingungenVersuchsvorschriftAufarbeitungQuellen und NachweiseNotizen zur Reaktion