Diethylamine → HCID 178457155, Verbindung

HRID 605504

Reaktionsgleichung

Reaktionsgleichung von HRID 605504
[I-:1].[I-].[I-].[CH2:4]([N:7]([C:11]1[CH:12]=[CH:13][C:14]2[C:23]([CH:24]=1)=[S+:22][C:21]1[C:16](=[CH:17][CH:18]=[CH:19][CH:20]=1)[N:15]=2)[CH2:8][CH2:9][CH3:10])[CH2:5][CH3:6].[CH2:25]([N:28](C1C=CC2C(C=1)=[S+]C1C(=CC=CC=1)N=2)[CH2:29][CH2:30]C)[CH2:26]C.C(N(C1C=CC2C(C=1)=[S+]C1C(=CC=CC=1)N=2)CCC)CC.C(NCC)C>>[I-:1].[CH2:25]([N:28]([C:19]1[CH:18]=[CH:17][C:16]2[C:21]([CH:20]=1)=[S+:22][C:23]1[C:14](=[CH:13][CH:12]=[C:11]([N:7]([CH2:8][CH2:9][CH3:10])[CH2:4][CH2:5][CH3:6])[CH:24]=1)[N:15]=2)[CH2:29][CH3:30])[CH3:26]

Komponenten

3

Edukt 2

HCID 8021DiethylamineHCID 178457153HCID 178457153, Verbindung

Produkt 1

HCID 178457155HCID 178457155, Verbindung

Versuchsvorschrift

This compound was obtained following isolation of 3-(N,N-dipropylamino)-phenothiazin-5-ium triiodide and subsequent treatment with diethylamine. Precipitation from dichloromethane by addition of diethyl ether yielded purple lustrous crystals. Mass spectrometry: C22H30N3OS requires m/z=368; found m/z=368 (I− not detected by mass spectrometry).

Aufarbeitung

  1. customThis compound was obtained
  2. customPrecipitation from dichloromethane
  3. additionby addition of diethyl ether yielded purple lustrous crystals

Quellen und Nachweise

ORD-Eintrag
ord-4bee954ffb85427e8508dab56d815673
Quelldatensatz
uspto-grants-2011_03
Patentnummer
US07915254B2

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