HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Hydrochloric Acid → 5-Methyl-2-(pyridin-4-yl)benzoic acid hydrochloride
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Hydrochloric Acid | HCID 313 | — |
| Edukt | Methyl 5-methyl-2-(pyridin-4-yl)benzoate | HCID 86680841 | — |
| Lösungsmittel | Acetic Acid | HCID 176 | — |
| Produkt | 5-Methyl-2-(pyridin-4-yl)benzoic acid hydrochloride | HCID 86680842 | — |
Reaktionsschritte
A mixture of methyl 5-methyl-2-(pyridin-4-yl)benzoate (8.8 g), 6 N hydrochloric acid (65 mL) and acetic acid (100 mL) was heated under reflux overnight. The solvent was evaporated under reduced pressure, and the obtained solid was washed with ethyl acetate to give the title compound (6.6 g).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US09440990B2 |
| Quelldatensatz | uspto-grants-2016_09 |
| ORD ID | ord-af2844a64cfa403e89abd8269f3bd4d6 |
| Quellennotiz | uspto-grants-2016_09 |