Hydrochloric Acid → 2-Chloro-2-methyl-3-nitrosopentane

Temperatur

-20 °C

Dry hydrogen chloride gas was passed into a mixture of 2-methyl-2-pentene (20 g, 237 mmol) and iso-amyl nitrite (55.67 g, 475 mmol) cooled to -20° C. The reaction mixture was left to stir at 0° C. overnight and the precipitated material was then filtered off and washed with cold (-20° C.) ethanol (3×5 ml). The product was dried in a stream of air and was used without further purification, (13 g, 36%).

1. waitThe reaction mixture was left
2. filtrationthe precipitated material was then filtered off
3. washwashed with cold (-20° C.) ethanol (3×5 ml)
4. customThe product was dried in a stream of air
5. customwas used without further purification, (13 g, 36%)

ORD-Eintrag

ord-05e94ea8f0d644f3b3c8be9d4ebb5bb0

Quelldatensatz

uspto-grants-1999_12

DOI

10.6084/m9.figshare.5104873.v1

Patentnummer

US05997843