HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
(1-Butylpiperidin-4-yl)methanol → (1-n Butyl-4-piperidyl)methyl 5-fluoroindole-3-carboxylate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | (1-Butylpiperidin-4-yl)methanol | HCID 10241250 | — |
| Edukt | 5-Fluoroindole-3-carboxylic acid chloride | HCID 54328249 | — |
| Produkt | (1-n Butyl-4-piperidyl)methyl 5-fluoroindole-3-carboxylate | HCID 53920547 | 30% |
Reaktionsschritte
5-Fluoroindole-3-carboxylic acid chloride was reacted with (1-n butyl-4-piperidyl)methanol (D6) using the method of Example 1a to afford (1-n butyl -4-piperidyl)methyl 5-fluoroindole-3-carboxylate as an orange oil (30%), following flash chromatography on silica gel eluting with 10% ethanol/chloroform.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05998409 |
| Quelldatensatz | uspto-grants-1999_12 |
| ORD ID | ord-6bdb956acca849a29fee6c8b703316c2 |
| Quellennotiz | uspto-grants-1999_12 |