3-Nitrobenzanilide → 3-Aminobenzanilide

Beteiligte Stoffe

Reaktionsschritte

10% Palladium on carbon (2.0 g) was added to a solution of 3-nitro-N-phenyl-benzamide (20 g, 83 mmol) in ethanol (225 mL) and the mixture was hydrogenated at 45 psi for 2 hours. The mixture was filtered through diatomaceous earth and concentrated to give a colorless solid (mp 118-120° C., 16 g, 90%).

Herkunft & Nachweise