HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Acetate → HCID 66870991, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Acetate | HCID 175 | — |
| Edukt | Terephthalic Acid | HCID 7489 | — |
| Edukt | Formic acid, copper salt | HCID 44152240 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Produkt | HCID 66870991 | HCID 66870991 | 42,4% |
Reaktionsschritte
0.70 g of terephthalic acid was dissolved under heating in a mixture solvent of 400 cm3 of methanol and 20 cm3 of acetate. After this solution was cooled to the normal temperature, into this solution, a further solution in which 0.95 g of formic acid copper was dissolved in 50 cm3 of methanol was dripped and then this was kept still for a few days. Thereafter, the precipitation product was suction-filtered and dried for 110° C./4 hours, whereby 0.41 g of terephthalic acid copper was obtained.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05998647 |
| Quelldatensatz | uspto-grants-1999_12 |
| ORD ID | ord-540d390b47ce4090addbea88f06ffda2 |
| Quellennotiz | uspto-grants-1999_12 |