Hydrochloric Acid → 1-(2-diethylaminomethyl-5,7-dihydro-4H-furo[2,3-c]pyridin-6-yl)-6-phenylhexan-1-one hydrochloride

HRID 611173

Reaktionsgleichung

Reaktionsgleichung von HRID 611173
[CH2:1]([N:3]([CH2:6][C:7]1[O:28][C:10]2[CH2:11][N:12]([C:15](=[O:27])[CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][C:21]3[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=3)[CH2:13][CH2:14][C:9]=2[CH:8]=1)[CH2:4][CH3:5])[CH3:2].[ClH:29]>CO>[ClH:29].[CH2:1]([N:3]([CH2:6][C:7]1[O:28][C:10]2[CH2:11][N:12]([C:15](=[O:27])[CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][C:21]3[CH:22]=[CH:23][CH:24]=[CH:25][CH:26]=3)[CH2:13][CH2:14][C:9]=2[CH:8]=1)[CH2:4][CH3:5])[CH3:2]

Komponenten

4

Edukt 2

HCID 313Hydrochloric AcidHCID 196001221-(2-diethylaminomethyl-5,7-dihydro-4H-furo[2,3-c]pyridin-6-yl)-6-phenylhexan-1-one

Produkt 1

HCID 196001211-(2-diethylaminomethyl-5,7-dihydro-4H-furo[2,3-c]pyridin-6-yl)-6-phenylhexan-1-one hydrochloride

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 887MethanolLösungsmittel2×

Versuchsvorschrift

1-(2-Diethylaminomethyl-5,7-dihydro-4H-furo[2,3-c]pyridin-6-yl)-6-phenylhexan-1-one 0.178 g was dissolved in 2 ml of methanol; hydrogen chloride in methanol was added in excess, followed by stirring. This mixture was concentrated to yield the desired product.

Aufarbeitung

  1. concentrationThis mixture was concentrated

Quellen und Nachweise

ORD-Eintrag
ord-404ee9f641344e9bb502b6be92848703
Quelldatensatz
uspto-grants-1999_12
Patentnummer
US05998433

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