Hydrochloric Acid → HCID 19600026, Verbindung

HRID 611212Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 611212
[CH3:1][N:2]([CH2:4][C:5]1[O:13][C:12]2[CH2:11][CH2:10][N:9]([S:14]([CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][C:22]3[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=3)(=[O:16])=[O:15])[CH2:8][C:7]=2[CH:6]=1)[CH3:3].[ClH:28]>CO>[ClH:28].[CH3:1][N:2]([CH2:4][C:5]1[O:13][C:12]2[CH2:11][CH2:10][N:9]([S:14]([CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][C:22]3[CH:23]=[CH:24][CH:25]=[CH:26][CH:27]=3)(=[O:16])=[O:15])[CH2:8][C:7]=2[CH:6]=1)[CH3:3]

Komponenten

4

Edukt 2

HCID 313Hydrochloric AcidHCID 19599983HCID 19599983, Verbindung

Produkt 1

HCID 19600026HCID 19600026, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 887MethanolLösungsmittel2×

Versuchsvorschrift

N,N-Dimethyl-[5-(5-phenylpentylsulfonyl)-4,5,6,7-tetrahydrofuro[3,2-c]pyridin-2-ylmethyl]amine 0.244 g was dissolved in 2 ml of methanol; hydrogen chloride in methanol was added in excess, followed by stirring. After this mixture was concentrated, diethyl ether was added; the resulting solid was filtered and washed with diethyl ether to yield the desired product.

Aufarbeitung

  1. concentrationAfter this mixture was concentrated
  2. additiondiethyl ether was added
  3. filtrationthe resulting solid was filtered
  4. washwashed with diethyl ether

Quellen und Nachweise

ORD-Eintrag
ord-74ff4d90d44447cea414b9d38c3bec47
Quelldatensatz
uspto-grants-1999_12
Patentnummer
US05998433

Notizen zur Reaktion

Wird geladen…