Hydrochloric Acid → 2-dimethylaminomethyl-5-(6-phenylhexyl)-6,7-dihydro-5H-furo[3,2-c]pyridin-4-one hydrochloride

HRID 611431Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 611431
[CH3:1][N:2]([CH2:4][C:5]1[O:13][C:12]2[CH2:11][CH2:10][N:9]([CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][C:20]3[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=3)[C:8](=[O:26])[C:7]=2[CH:6]=1)[CH3:3].[ClH:27]>CO>[ClH:27].[CH3:1][N:2]([CH2:4][C:5]1[O:13][C:12]2[CH2:11][CH2:10][N:9]([CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][C:20]3[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=3)[C:8](=[O:26])[C:7]=2[CH:6]=1)[CH3:3]

Komponenten

4

Edukt 2

HCID 313Hydrochloric AcidHCID 195999812-dimethylaminomethyl-5-(6-phenylhexyl)-6,7-dihydro-5H-furo[3,2-c]pyridin-4-one

Produkt 1

HCID 195999802-dimethylaminomethyl-5-(6-phenylhexyl)-6,7-dihydro-5H-furo[3,2-c]pyridin-4-one hydrochloride

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 887MethanolLösungsmittel2×

Versuchsvorschrift

2-Dimethylaminomethyl-5-(6-phenylhexyl)-6,7-dihydro-5H-furo[3,2-c]pyridin-4-one 0.159 g was dissolved in 2 ml of methanol; hydrogen chloride in methanol was added in excess, followed by stirring. This mixture was concentrated; the resulting solid was washed with diethyl ether to yield the desired product.

Aufarbeitung

  1. concentrationThis mixture was concentrated
  2. washthe resulting solid was washed with diethyl ether

Quellen und Nachweise

ORD-Eintrag
ord-9a234c6418aa446cbd082e10d9c24144
Quelldatensatz
uspto-grants-1999_12
Patentnummer
US05998433

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