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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 611650Erstellt: 26. Oktober 2026

Iodine → 2-[2-(Diethylamino)ethyl]-6-phenyl-isothiazolo[5,4-d]pyrimidin-3(2H)-one

https://huagongshe.com/reaction/611650

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktIodineHCID 807—
EduktHCID 178418472HCID 178418472—
Produkt2-[2-(Diethylamino)ethyl]-6-phenyl-isothiazolo[5,4-d]pyrimidin-3(2H)-oneHCID 990550368,5%

Reaktionsschritte

Using the procedure of Example 20, 3.3 g (0.01 mol) of 4-mercapto-2-phenyl-pyrimidine-5-carboxylic acid (2-diethylamino-ethyl)-amide (from Preparation 36) and 2.54 g (0.01 mol) of iodine were reacted to give 2.25 g of the title compound after recrystallization from isopropanol, mp 106-107° C.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS06001863
Quelldatensatzuspto-grants-1999_12
ORD IDord-8d3c4a6308d94507bb0a12f022de1457
Quellennotizuspto-grants-1999_12