HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Dimethylformamide → Dimethyl 4-phenoxyphthalate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Dimethylformamide | HCID 6228 | — |
| Edukt | Phenolate Sodium | HCID 4445035 | — |
| Edukt | HCID 19595681 | HCID 19595681 | — |
| Produkt | Dimethyl 4-phenoxyphthalate | HCID 19595677 | — |
Reaktionsschritte
Methyl 4-nitrophthalate was reacted in DMF with sodium phenoxide to give dimethyl 4-phenoxyphthalate in analogy to a process known from the literature (J. Org. Chem. Vol. 42, No. 21, 1977, 3419-3425). After standard working up and chromatography using hexane/EA, the diester was isolated as a yellowish oil.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06005010 |
| Quelldatensatz | uspto-grants-1999_12 |
| ORD ID | ord-fa7b70037ada4929a77540160665e705 |
| Quellennotiz | uspto-grants-1999_12 |