1,2-Ethanediamine, N1,N1-bis(1-methylethyl)- → N-[2-[Bis(1-methylethyl)amino]ethyl]-2-methyl-5-oxo-1-pyrrolidineacetamide

HRID 614480

Reaktionsgleichung

Reaktionsgleichung von HRID 614480
[CH3:1][CH:2]1[CH2:6][CH2:5][C:4](=[O:7])[N:3]1[CH2:8][C:9]([O:11]CC)=O.[CH:14]([N:17]([CH:21]([CH3:23])[CH3:22])[CH2:18][CH2:19][NH2:20])([CH3:16])[CH3:15]>>[CH3:15][CH:14]([N:17]([CH:21]([CH3:23])[CH3:22])[CH2:18][CH2:19][NH:20][C:9](=[O:11])[CH2:8][N:3]1[C:4](=[O:7])[CH2:5][CH2:6][CH:2]1[CH3:1])[CH3:16]

Komponenten

3

Edukt 2

HCID 84591,2-Ethanediamine, N1,N1-bis(1-methylethyl)-HCID 5744761-Pyrrolidineacetic acid, 2-methyl-5-oxo-, ethyl ester

Produkt 1

HCID 44374465N-[2-[Bis(1-methylethyl)amino]ethyl]-2-methyl-5-oxo-1-pyrrolidineacetamide

Versuchsvorschrift

From 9.2 g. of ethyl 2-methyl-5-oxo-1-pyrrolidineacetate and 8.7 g. of 2-(diisopropylamino)ethylamine, following the procedure of Example 9, there is obtained N-[2-[Bis(1-methylethyl)amino]ethyl]-2-methyl-5-oxo-1-pyrrolidineacetamide; m.p. 73°-74° C. after recrystallization from hexane.

Quellen und Nachweise

ORD-Eintrag
ord-4243bfd66dba4307827fc3fb5f394bb3
Quelldatensatz
uspto-grants-1979_03
Patentnummer
US04145347

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